Browsing by Author "Guedes, M."
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- 3D-Printing of zirconia dental prosthesesPublication . Rodrigues, I.; Olhero, S.; Guedes, M.; Serro, A. P.; Figueiredo-Pina, C. G.
- Book of Abstracts of 11th Iberian Conference on TribologyPublication . Serro, Ana Paula; Branco, Ana Catarina Branco; Carneiro, Carla; Silva, Diana; Guedes, M.; Figueiredo-Pina, Célio
- Effect of Fused Filament Fabrication Processing Parameters on The Mechanical Properties of PLA ComponentsPublication . Marat- Mendes, Rosa; Guedes, M.; Leite, M.; Baptista, R.
- Effect of Fused Filament Fabrication Processing Parameters on The Mechanical Properties of PLA ComponentsPublication . Marat-Mendes, R.; Guedes, M.; Leite, M.; Baptista, R.This paper studies the influence of Fused Filament Fabrication processing parameters upon mechanical properties and microstructural features of processed PLA parts. The effect of extrusion temperature and raster angle were tested upon two PLA filaments of different trademarks, DoWire and BQ, using a commercial fused deposition extruder. The filling density, layer thickness and velocity were kept constant at 60 %, 0.2 mm and 40 mm/s, respectively. Results allowed to determine fused filament fabrication parameters resulting in increased mechanical performance of manufactured parts. Mechanical performance is higher when material is stored under controlled atmosphere before use, and when material deposition direction is aligned with applied load. Increasing the extrusion temperature also increases performance, by increasing deformation ability of PLA molecules. Obtained results contribute to accumulation of a property database and provide design guidance to the procurement of additive manufacturing products with enhanced mechanical strength.
- Fatigue behavior of different geometry scaffolds for bone replacementPublication . Baptista, Ricardo; Guedes, M.When transplanting bone tissue is not a possibility, tissue engineering is responsible for developing solutions to substitute the functions of the missing bone structure or support the process of bone regeneration. Scaffolds can be used to fulfill this mission by supporting loads that were applied to the missing bone, supporting the cell regenerating process, allowing for the necessary nutrients and oxygen diffusion and delivering growth factors or drugs. Scaffold geometry design must support static and dynamic loads up to 20 MPa in order to replace human trabecular bone. Also, it should generate macro and micro pores to support cell growth and mineral precipitation, while all pores should be interconnected for nutrient and oxygen diffusion. Scaffolds were fabricated according to ASTM-695 standard, using two different layouts, 50% porosity and a theoretical distance of 0.8 mm between each filament. A 400 µm diameter nozzle was used, and scaffolds were produced at 215 ºC with deposition rate of 30 mm/s. Both designs were fatigue tested until 3600 cycles, using different load amplitudes and a frequency of 0.25 Hz. The orthogonal scaffold showed improved behavior, with compression modulus reaching 680 MPa, when a maximum stress of 14.5 MPa was applied.
- Processing of Copper-Graphite-Alumina Powders by High-Energy MillingPublication . Rodrigues, I.; Guedes, M.; Ferro, A. C.Copper-matrix composites are versatile materials used in several electromechanical applications, but relatively low strength and thermal stability impair advanced uses. Development of robust solutions combining low wear and low electrical loss are thus paramount. This work proposes high-energy milling of copper-graphite-alumina powders: graphite is conductive and self-lubricating; alumina toils as dispersion-strengthener and grain refiner. Tailored batches with 2wt%-graphite and 2wt%-alumina were milled up to 16h in planetary ball mill and characterized by XRD, FEG-SEM/EDS, microhardness and Raman. Produced powders are nanostructured, containing graphite and alumina nanoparticles homogeneously distributed in copper. Increasing milling time results in some degree of nanographite amorphization and size decrease. Copper crystallite size and achieved hardness are affected mainly above 4 h milling. Attained results suggest that efficient dispersion of graphite and alumina nanoparticles is achieved, envisaging high conductivity, high strength and thermal stability. The copper-graphite-alumina system thus seemingly opens an opportunity window for PM processing of advanced copper composites.
- Processing of near-net-shape dental crowns by conventional alumina slip casting in gypsum mouldPublication . Baptista, R.; Gonilho-Pereira, Cristiana; Marinho, R.; Grancho, S.; Ferro, A. C.; Guedes, M.
- Tribological behavior of unveneered and veneered lithium disilicate dental materialPublication . Figueiredo-Pina, C. G.; Patas, N.; Canhoto, J.; Cláudio, R.; Olhero, S.M.; Serro, A.P.; Ferro, A.C.; Guedes, M.The friction and wear behaviour of a lithium disilicate dental ceramic against natural dental enamel is studied, including the effect of the presence of a fluorapatite veneering upon the tribological properties of the material. The tribological behaviour was assessed using reciprocating pin-on-plate test configuration, at pH 3 and pH 7. The surface energy of the plates was determined, as well as the zeta potential of fluorapatite, lithium disilicate and enamel particles in artificial saliva. It was found that the friction and wear behaviour of the tested enamel/plate material tribocouples is less severe in unveneered plates. Initial surface roughness of the plate does not affect wear results. However the topography of the resulting wear track affects the corresponding wear loss: a smoother final wear track is associated with lower wear. The surface topography of the wear track, and thus the tribological performance of the tested materials, is very sensitive to the pH of the sliding solution. This is because the dissolution trend, wettability and surface charge of the used materials are pH dependent. Overall friction and wear are higher under basic pH conditions, especially when plates are veneered. A wear model is proposed that correlates the effect of the described parameters with the observed tribological behaviour at pH 7. Attained results show that fluorapatite coating of lithium disilicate dental crowns affects tooth/crown wear behaviour, resulting in increased wear of both the artificial crown and the opposing natural teeth. Coating should therefore be avoided in occlusal crown surfaces.