Repository logo
 
Publication

Multi-year inter-laboratory exercises for the analysis of illicit drugs and metabolites in wastewater:Development of a quality control system

2018Journal article Open access
Simple item page
dc.contributor.authorvan Nuijs, Alexander L.N.
dc.contributor.authorLai, Foon Yin
dc.contributor.authorBeen, Frederic
dc.contributor.authorAndres-Costa, Maria Jesus
dc.contributor.authorBarron, Leon
dc.contributor.authorBaz-Lomba, Jose Antonio
dc.contributor.authorBerset, Jean-Daniel
dc.contributor.authorBenaglia, Lisa
dc.contributor.authorBijlsma, Lubertus
dc.contributor.authorBurgard, Dan
dc.contributor.authorCastiglioni, Sara
dc.contributor.authorChristophoridis, Christophoros
dc.contributor.authorCovaci, Adrian
dc.contributor.authorde Voogt, Pim
dc.contributor.authorEmke, Erik
dc.contributor.authorFatta-Kassinos, Despo
dc.contributor.authorFick, Jerker
dc.contributor.authorHernandez, Felix
dc.contributor.authorGerber, Cobus
dc.contributor.authorGonzález-Mariño, Iria
dc.contributor.authorGrabic, Roman
dc.contributor.authorGunnar, Teemu
dc.contributor.authorKannan, Kurunthachalam
dc.contributor.authorKarolak, Sara
dc.contributor.authorKasprzyk-Hordern, Barbara
dc.contributor.authorKokot, Zenon
dc.contributor.authorKrizman-Matasic, Ivona
dc.contributor.authorLi, Angela
dc.contributor.authorLi, Xiqing
dc.contributor.authorLöve, Arndís S.C.
dc.contributor.authorLopez de Alda, Miren
dc.contributor.authorMcCall, Ann-Kathrin
dc.contributor.authorMeyer, Markus R.
dc.contributor.authorOberacher, Herbert
dc.contributor.authorO'Brien, Jake
dc.contributor.authorQuintana, Jose Benito
dc.contributor.authorReid, Malcolm
dc.contributor.authorSchneider, Serge
dc.contributor.authorSimões, Susana
dc.contributor.authorThomaidis, Nikolaos S.
dc.contributor.authorThomas, Kevin
dc.contributor.authorYargeau, Viviane
dc.contributor.authorOrt, Christoph
dc.date.accessioned2021-08-11T10:36:52Z
dc.date.available2021-08-11T10:36:52Z
dc.date.issued2018
dc.description.abstractThis study presents the development of a worldwide inter-laboratory testing scheme for the analysis of seven illicit drug residues in different matrices (standard solutions, tap- and wastewater). By repeating this exercise for six years with participation of 37 laboratories from 25 countries, the testing scheme was substantially improved based on experiences gained across the years (e.g. matrix type, sample conditions, spiking levels). From the exercises, (pre-)analytical issues (e.g. pH adjustment, filtration) were revealed for some analytes which resulted in formulation of best- practice protocols, both for inter-laboratory setup and analytical procedures. The results illustrate the effectiveness of the inter-laboratory testing scheme in assessing laboratory performance in the framework of illicit drug analysis in wastewater. The exercise proved that measurements of laboratories were of high quality (> 80% satisfactory results for 6 out of 7 analytes) and that analytical follow-up is important to assist laboratories in improving robustness of wastewater-based epidemiology results.pt_PT
dc.description.versioninfo:eu-repo/semantics/acceptedVersionpt_PT
dc.identifier.citationvan Nuijs, A. L. N., Lai, F. Y., Been, F., Jesus Andres-Costa, M., Barron, L., Baz-Lomba, J. A., Berset, J-D., Benaglia, L., Bijlsma, L., Burgard, D., Castiglioni, S., Christophoridis, C., Covaci, A., de Voogt, P., Emke, E., Fatta-Kassinos, D., Fick, J., Hernandez, F., Gerber, C., ... Ort, C. (2018). Multi-year interlaboratory exercises for the analysis of illicit drugs and metabolites in wastewater: development of a quality control system. TRENDS IN ANALYTICAL CHEMISTRY. https://doi.org/10.1016/j.trac.2018.03.009pt_PT
dc.identifier.doi10.1016/j.trac.2018.03.009pt_PT
dc.identifier.issn0165-9936
dc.identifier.urihttp://hdl.handle.net/10400.26/37293
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherElsevierpt_PT
dc.relation.publisherversionhttps://www.sciencedirect.com/science/article/pii/S0165993617303667pt_PT
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/pt_PT
dc.subjectWastewaterpt_PT
dc.subjectIllicit drugspt_PT
dc.subjectInter-laboratory testingpt_PT
dc.subjectWastewater-based epidemiologypt_PT
dc.subjectQuality assurancept_PT
dc.titleMulti-year inter-laboratory exercises for the analysis of illicit drugs and metabolites in wastewater:Development of a quality control systempt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.citation.endPage43pt_PT
oaire.citation.startPage34pt_PT
oaire.citation.titleTrAC Trends in Analytical Chemistrypt_PT
oaire.citation.volume103pt_PT
person.familyNameSimões
person.givenNameSusana
person.identifier.orcid0000-0002-9457-1546
rcaap.rightsopenAccesspt_PT
rcaap.typearticlept_PT
relation.isAuthorOfPublicationd0a1e3e3-4d0e-49b5-804e-a55e700f8d22
relation.isAuthorOfPublication.latestForDiscoveryd0a1e3e3-4d0e-49b5-804e-a55e700f8d22

Files

Original bundle
Now showing 1 - 1 of 1
Thumbnail Image
Name:
Multi-year interlaboratory exercises for the analysis.pdf
Size:
1.43 MB
Format:
Adobe Portable Document Format
Download

Collections

INMLCF - Artigos Científicos