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Recent Trends in Solid-Phase Microextraction for the Monitoring of Drugs of Abuse in Wastewater

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datacite.subject.fosCiências Naturais::Ciências Químicas
dc.contributor.authorDias Dinis, Pedro Alexandre
dc.contributor.authorGallardo, Eugenia
dc.contributor.authorMargalho, Cláudia
dc.date.accessioned2026-01-23T18:50:44Z
dc.date.available2026-01-23T18:50:44Z
dc.date.issued2025
dc.description.abstractWastewater analysis plays a central role in monitoring patterns of drug use within specific populations. It provides objective and real-time estimates of consumption, with minimal ethical concerns. In the current European context, drugs of abuse continue to be detected in wastewater, with varying incidences across countries. Their monitoring enables the prioritisation of public health and legal interventions by healthcare professionals and drug monitoring agencies. Therefore, the development and implementation of efficient methodologies for monitoring drugs of abuse in wastewater samples is of critical importance. This systematic review aims to explore the use of miniaturised sample extraction techniques based on solid-phase microextraction for the determination of drugs of abuse in wastewater. In fact, the extraction procedure must be fast, effective, and selective in order to retain the analytes of interest. Miniaturised techniques have thus emerged as promising alternatives to conventional methods. Magnetic solid-phase extraction (MSPE) and molecularly imprinted polymers (MIPs) represent the most widely applied solid-phase microextraction techniques in recent years for the analysis of drugs of abuse in wastewater. Looking ahead, future perspectives include the development of eco-friendly workflows, automated and time-efficient techniques, increasingly selective sorbents, and robust analytical methods.eng
dc.identifier.citationDinis, P.; Gallardo, E.; Margalho, C. Recent Trends in Solid-Phase Microextraction for the Monitoring of Drugs of Abuse in Wastewater. Separations 2025, 12, 256.
dc.identifier.doihttps://doi.org/10.3390/separations12090256
dc.identifier.issn2297-8739
dc.identifier.urihttp://hdl.handle.net/10400.26/61166
dc.language.isoeng
dc.peerreviewedyes
dc.publisherMDPI
dc.relation.hasversionhttps://doi.org/10.3390/separations12090256
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/
dc.subjectsolid-phase microextraction
dc.subjectSPME
dc.subjectMSPE
dc.subjectMIPs
dc.subjectdrugs of abuse
dc.subjectillicit drugs
dc.subjectwastewater
dc.subjectGC-MS
dc.subjectLC-MS/MS
dc.titleRecent Trends in Solid-Phase Microextraction for the Monitoring of Drugs of Abuse in Wastewatereng
dc.typereview article
dspace.entity.typePublication
oaire.citation.endPage24
oaire.citation.issue256
oaire.citation.startPage1
oaire.citation.titleSeparations
oaire.citation.volume12
oaire.versionhttp://purl.org/coar/version/c_970fb48d4fbd8a85
person.familyNameDias Dinis
person.familyNameGallardo
person.familyNameMargalho
person.givenNamePedro Alexandre
person.givenNameEugenia
person.givenNameCláudia
person.identifier.ciencia-id1A17-DAC1-3C27
person.identifier.ciencia-idF617-5CA5-EF61
person.identifier.ciencia-idA211-521D-90CA
person.identifier.orcid0009-0007-5443-1411
person.identifier.orcid0000-0002-1802-8998
person.identifier.orcid0000-0003-1661-0367
person.identifier.ridKII-2916-2024
person.identifier.scopus-author-id8655072100
relation.isAuthorOfPublicationc6f87a02-1078-4e3b-9cf1-2e49e195f7de
relation.isAuthorOfPublicationdde2079f-5556-4f43-8253-77bd51c001fe
relation.isAuthorOfPublication267f4998-7eea-4d9f-9216-8adcd52fbe1f
relation.isAuthorOfPublication.latestForDiscoveryc6f87a02-1078-4e3b-9cf1-2e49e195f7de

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